HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
n-Cyclohexylpiperidine-4-carboxamide → HCID 86706526, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | n-Cyclohexylpiperidine-4-carboxamide | HCID 12410238 | — |
| Edukt | 2-Chloro-3-nitrobenzaldehyde | HCID 12667713 | — |
| Edukt | 1-(2-Chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide | HCID 86706527 | — |
| Produkt | HCID 86706526 | HCID 86706526 | — |
Reaktionsschritte
The title compound is prepared according to the reactions described above starting from 2-chloro-3-nitro-benzaldehyde and piperidine-4-carboxylic acid cyclohexylamide giving after reductive amination 1-(2-chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide LC-MS B: tR=0.57 min; [M+H]+=380.14 and reduction with stannous chloride the title compound LC-MS A: tR=0.50 min; [M+H]+=350.20.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09428456B2 |
| Quelldatensatz | uspto-grants-2016_08 |
| ORD ID | ord-f2b5c8cf9e8b451690eb334efb45e56a |
| Quellennotiz | uspto-grants-2016_08 |