HRID1486697

反应详情

EQUATION

反应方程式

HRID 1486697 的结构方程式

PROCEDURE

实验过程

The title compound is prepared according to the reactions described above starting from 2-chloro-3-nitro-benzaldehyde and piperidine-4-carboxylic acid cyclohexylamide giving after reductive amination 1-(2-chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide LC-MS B: tR=0.57 min; [M+H]+=380.14 and reduction with stannous chloride the title compound LC-MS A: tR=0.50 min; [M+H]+=350.20.

WORKUP

后处理

  1. customThe title compound is prepared