Butyl Isothiocyanate → 1-(n-Butyl)-3-(2-morpholinophenyl)thiourea

Beteiligte Stoffe

Reaktionsschritte

A solution of 4-(2-aminophenyl)morpholine (5.8 g) in dichloromethane (60 ml) was treated with n-butyl isothiocyanate (5 g) and mixture stirred at room temperature for 4 days to yield 1-(n-butyl)-3-(2-morpholinophenyl)thiourea as a pale yellow solid (m.p. 105° C.).

Herkunft & Nachweise