Triethylamine → HCID 118380271, Verbindung
Reaktionsgleichung
[C:1]([N:8]([CH2:12][CH2:13][OH:14])[CH2:9][CH2:10][OH:11])([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2].C(N(CC)CC)C.Cl[C:23](Cl)([O:25]C(=O)OC(Cl)(Cl)Cl)Cl>ClCCl>[C:1]([N:8]1[CH2:9][CH2:10][O:11][C:23](=[O:25])[O:14][CH2:13][CH2:12]1)([O:3][C:4]([CH3:6])([CH3:7])[CH3:5])=[O:2]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The procedure of Example 1 was followed using N-boc diethanolamine (3 g, 14.6 mmol), triethylamine (4.1 mL, 29.2 mmol), dry dichloromethane (100 mL) and triphosgene (1.4 g, 4.9 mmol). The filtrate was concentrated yielding only oligomeric compounds.
Aufarbeitung
- concentrationThe filtrate was concentrated
- customyielding only oligomeric compounds
Quellen und Nachweise
- ORD-Eintrag
- ord-e881160028974952840763b6267931ac
- Quelldatensatz
- uspto-grants-2015_12
- Patentnummer
- US09215876B2
Notizen zur Reaktion
Wird geladen…