HCID 178476752, Verbindung → Zinc Acetate
Reaktionsgleichung
[Zn:1](OC(C)=O)[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[C:3]([O-:4])(=[O:2])[CH3:5].[Zn+2:1].[C:3]([O-:4])(=[O:2])[CH3:5]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
83.7 g of MeOH was added to Zn(OAc)2.2H2O (19.88 g) in a beaker to form 0.85 mol/L zinc acetate solution. 12.72 g of concentrated NaOH aqueous solution (49.8 wt %) was diluted with 83.7 g of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 4 minutes after the NaOH solution was mixed with the Zn(OAc)2 solution, 80 mL of 0.05 mol/L sodium oleate aqueous solution was added to the reaction solution. White precipitate formed almost immediately after the addition of sodium oleate. The reaction solution was aged at 62° C. for 45 minutes.
Quellen und Nachweise
- ORD-Eintrag
- ord-ee568a6d4aea49a2bf4e62db318f8359
- Quelldatensatz
- uspto-grants-2015_07
- Patentnummer
- US09090468B2
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