Hydrochloric Acid → HCID 19908400, Verbindung

HRID 1534844Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1534844
[O-:1][C:2]#[N:3].[K+].[C:5]([NH:10][NH2:11])([CH2:8][CH3:9])([CH3:7])[CH3:6].Cl>O>[C:5]([NH:10][NH:11][C:2]([NH2:3])=[O:1])([CH2:8][CH3:9])([CH3:7])[CH3:6]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 117546HCID 117546, VerbindungHCID 11378442Potassium cyanate

Produkt 1

HCID 19908400HCID 19908400, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

13.6 g of potassium cyanate are added to a mixture of 17 g of tert-pentylhydrazine and 30 ml of water cooled in an ice bath and 16.5 g of conc. hydrochloric acid are then added dropwise. The mixture is stirred at room temperature for 3 h and the solid is filtered off with suction, washed with water and dried in vacuo.

Aufarbeitung

  1. temperaturecooled in an ice bath
  2. filtrationthe solid is filtered off with suction
  3. washwashed with water
  4. customdried in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-4d8ee08daba343dfb7c4cd34613a8364
Quelldatensatz
uspto-grants-1992_02
Patentnummer
US05091398

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