Hydrochloric Acid → Sulfanilamide Hydrochloric Acid Brij 35

HRID 1578220

Reaktionsgleichung

Reaktionsgleichung von HRID 1578220
[S:1]([NH2:11])(=[O:10])([C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1)=[O:2].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27].[ClH:28]>O>[S:1]([NH2:11])(=[O:10])([C:3]1[CH:4]=[CH:5][C:6]([NH2:9])=[CH:7][CH:8]=1)=[O:2].[ClH:28].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 5333Sulfanilamide2×HCID 247502-(Dodecyloxy)ethanol

Produkt 1

HCID 131712428Sulfanilamide Hydrochloric Acid Brij 35

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel2×

Versuchsvorschrift

To a 2 liter volumetric flask containing approximately 1500 ml. of distilled water is added 20.0 g. of sulfanilamide (0.116 mol), 66 ml. of Brij 35 and 200 ml. of concentrated hydrochloric acid. The resulting mixture is taken up to 2 liters with distilled water and then stirred until the sulfanilamide is completely dissolved.

Aufarbeitung

  1. additionTo a 2 liter volumetric flask containing approximately 1500 ml
  2. dissolutionis completely dissolved

Quellen und Nachweise

ORD-Eintrag
ord-5bde5d665a8e41d9bcf7e6b78f5c52a5
Quelldatensatz
uspto-grants-1981_09
Patentnummer
US04292040

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