Formaldehyde → 4,5-Dihydroxy-1-(hydroxymethyl)imidazolidin-2-one

HRID 1578228

Reaktionsgleichung

Reaktionsgleichung von HRID 1578228
[CH2:1]=[O:2].[CH:3]1([OH:10])[NH:8][C:6](=[O:7])[NH:5][CH:4]1[OH:9]>O>[CH2:1]([N:5]1[CH:4]([OH:9])[CH:3]([OH:10])[NH:8][C:6]1=[O:7])[OH:2]

Komponenten

4

Edukt 2

HCID 712FormaldehydeHCID 979152-Imidazolidinone, 4,5-dihydroxy-

Produkt 1

HCID 893644,5-Dihydroxy-1-(hydroxymethyl)imidazolidin-2-one

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
55 °C

Versuchsvorschrift

Formaldehyde (8.85 parts of 37.3 percent solution; 0.11 mole), adjusted to pH 7-8.5, is diluted with water (20 parts). While stirring, 11.8 parts (0.1 mole) of dihydroxyethyleneurea powder are added. The temperature is raised to 55° C., held at 55° C. for 30 minutes, cooled to room temperature, and refrigerated. The sample is recovered as an 80 percent aqueous solution.

Aufarbeitung

  1. temperaturecooled to room temperature
  2. customThe sample is recovered as an 80 percent aqueous solution

Quellen und Nachweise

ORD-Eintrag
ord-a880f1b71a6543c08b181ef66b99b994
Quelldatensatz
uspto-grants-1981_09
Patentnummer
US04292111

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