Reaktionsgleichung
[C:1]([C:4]1[CH:16]=[CH:15][C:14]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[CH2:7][C:6]=2[CH:5]=1)(=[O:3])[CH3:2].C(C1C=CC2OC3C=CC=CC=3C=2C=1)(=O)C.[N:33]1[CH2:37][CH2:36][CH2:35][CH:34]=1.N1CCCCC=1>>[NH:33]1[CH2:37][CH2:36][CH2:35][CH:34]1[CH2:2][C:1]([C:4]1[CH:16]=[CH:15][C:14]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[CH2:7][C:6]=2[CH:5]=1)=[O:3]Komponenten
5
Versuchsvorschrift
Following essentially the same procedure as in Example XI above, but substituting 2-acetylfluorene for the 2-acetyldibenzofuran above and substituting 1-pyrroline as the trimer for the 2,3,4,5-tetrahydropyridine (as α-tripiperidein) above results in the formation of 2-fluorenyl 2-pyrrolidinylmethyl ketone as the hydrochloride salt, and which when recrystallized from isopropyl alcohol has a M.P. of 234-44°C. (dec.)
Quellen und Nachweise
- ORD-Eintrag
- ord-fb20cab4092b4b5e843807665404280b
- Quelldatensatz
- uspto-grants-1976_01
- Patentnummer
- US03931155
Verknüpfte Notizen
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