HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Alcohol → HCID 178476834, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Alcohol | HCID 244 | — |
| Edukt | Water | HCID 962 | — |
| Edukt | HCID 178476830 | HCID 178476830 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | HCID 178476834 | HCID 178476834 | 91,2% |
Reaktionsschritte
A solution of α-hydroxyethylphosphinic acid (5.5 g) and benzyl alcohol (2.26 g) in benzene (50 ml) was heated for 8 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 3.65 g (91.2%) of benzyl α-hydroxyethylphosphinate (Compound No. 36).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04554111 |
| Quelldatensatz | uspto-grants-1985_11 |
| ORD ID | ord-16302dc960c74e4580f5028245e59782 |
| Quellennotiz | uspto-grants-1985_11 |