HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glycine → O-Benzyl-N-(tert-butoxycarbonyl)-L-serylglycine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glycine | HCID 750 | — |
| Edukt | Sodium Bicarbonate | HCID 516892 | — |
| Edukt | Boc-Ser(Bzl)-OSu | HCID 12879025 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | O-Benzyl-N-(tert-butoxycarbonyl)-L-serylglycine | HCID 14608022 | — |
Reaktionsschritte
To an aqueous solution containing 6.80 g of H-Gly-OH and 9.20 g of sodium hydrogen carbonate, under ice-cooling condition, was added 120 ml of THF solution containing 27.5 g of Boc-Ser(Bzl)-OSu, and the mixture was stirred at room temperature overnight.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05204326 |
| Quelldatensatz | uspto-grants-1993_04 |
| ORD ID | ord-f981639275ce4afcb212119f5339d2a8 |
| Quellennotiz | uspto-grants-1993_04 |