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HRID1590967

反应详情

EQUATION

反应方程式

HRID 1590967 的结构方程式

REACTANTS

反应物

3
结构：NCC(=O)O
HCID750

Glycine

C2H5NO2

结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：CC(C)(C)OC(=O)N[C@@H](COCc1ccccc1)C(=O)ON1C(=O)CCC1=O
HCID12879025

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@@H](COCc1ccccc1)C(=O)NCC(=O)O
HCID14608022

O-Benzyl-N-(tert-butoxycarbonyl)-L-serylglycine

C17H24N2O6

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

To an aqueous solution containing 6.80 g of H-Gly-OH and 9.20 g of sodium hydrogen carbonate, under ice-cooling condition, was added 120 ml of THF solution containing 27.5 g of Boc-Ser(Bzl)-OSu, and the mixture was stirred at room temperature overnight.

WORKUP

后处理

  1. temperatureunder ice-cooling condition