4-Toluenesulfonyl chloride → (RS)-1-(Toluene-4-sulfonyl)-2-m-tolyl-pyrrolidine
Reaktionsgleichung
[C:1]1([CH3:12])[CH:6]=[CH:5][CH:4]=[C:3]([CH:7]2[CH2:11][CH2:10][CH2:9][NH:8]2)[CH:2]=1.[C:13]1([CH3:23])[CH:18]=[CH:17][C:16]([S:19](Cl)(=[O:21])=[O:20])=[CH:15][CH:14]=1>>[C:13]1([CH3:23])[CH:18]=[CH:17][C:16]([S:19]([N:8]2[CH2:9][CH2:10][CH2:11][CH:7]2[C:3]2[CH:2]=[C:1]([CH3:12])[CH:6]=[CH:5][CH:4]=2)(=[O:21])=[O:20])=[CH:15][CH:14]=1Komponenten
3
Versuchsvorschrift
The title compound, off-white solid, m.p. 79° C. and MS: m/e=315 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-m-tolyl-pyrrolidine and toluene-4-sulfonyl chloride.
Quellen und Nachweise
- ORD-Eintrag
- ord-df6ff040b81445c4bb0ef6795d616176
- Quelldatensatz
- uspto-grants-2001_09
- Patentnummer
- US06284785B1
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