HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Fluoroaniline → Methyl 4-(2-fluorophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Fluoroaniline | HCID 9584 | — |
| Edukt | Methyl 4-chloro-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate | HCID 57886211 | — |
| Produkt | Methyl 4-(2-fluorophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate | HCID 66674390 | 61% |
Reaktionsschritte
The title compound was prepared in 61% yield by the procedure as previously described in Example 166 (step H) using methyl 4-chloro-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate (109 mg, 0.54 mmol, prepared as previously described in Example 1 (steps A-G) and 2-fluoroaniline (0.053 mL, 0.54 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732616B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-e3d3226b93d840e1a9ed91970ad037b0 |
| Quellennotiz | uspto-grants-2010_06 |