Oxalyl chloride → 3-(4-Methylphenyl)propanoyl chloride

HRID 1599471Notizen

Reaktionsgleichung

[C:1](Cl)(=O)[C:2]([Cl:4])=[O:3].[CH3:7][C:8]1[CH:13]=[CH:12][C:11]([CH2:14]CC(O)=O)=[CH:10][CH:9]=1>ClCCl>[CH3:7][C:8]1[CH:13]=[CH:12][C:11]([CH2:14][CH2:1][C:2]([Cl:4])=[O:3])=[CH:10][CH:9]=1

Komponenten

Reaktionsbedingungen

Temperatur: 20 °C

Versuchsvorschrift

A solution of oxalyl chloride (5 ml) in dichloromethane (5 ml) was added dropwise to a solution of 3-(4-methylphenyl)propionic acid (1.5 g) in dichloromethane (20 ml). The mixture was stirred at 20° C. for 16 hours and then evaporated to give 3-(4-methylphenyl)propionyl chloride as an oil.

Aufarbeitung

customevaporated

Quellen und Nachweise

ORD-Eintrag: ord-8003302ee8fe4e75926472882c33d452
Quelldatensatz: uspto-grants-1998_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05741800

Notizen zur Reaktion

Wird geladen…