1-Butanaminium, N,N,N-tributyl-, azide → Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester

HRID 1600102

Reaktionsgleichung

Reaktionsgleichung von HRID 1600102
FC(F)(F)S(O[CH2:7][C@H:8]1[O:12][CH2:11][C@@H:10]([S:13][C:14](=[O:16])[CH3:15])[CH2:9]1)(=O)=O.[N-:19]=[N+:20]=[N-:21].C([N+](CCCC)(CCCC)CCCC)CCC>C(Cl)Cl>[N:19]([CH2:7][C@H:8]1[O:12][CH2:11][C@@H:10]([S:13][C:14](=[O:16])[CH3:15])[CH2:9]1)=[N+:20]=[N-:21]

Komponenten

4

Versuchsvorschrift

The title compound is prepared by the procedure of Example 43 using 0.560 gof product from Example 60 in 2 ml of methylene chloride, 0.569 g of tetrabutylammonium azide in 2 ml of methylene chloride to give 0.321 g of the desired product.

Quellen und Nachweise

ORD-Eintrag
ord-d6b5432746c04169951918d91df29c50
Quelldatensatz
uspto-grants-1998_04
Patentnummer
US05744465

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