HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Imidazole → Diethyl 3-(tert-Butyldimethylsilyloxy)glutarate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Imidazole | HCID 795 | — |
| Edukt | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Edukt | Diethyl 3-hydroxyglutarate | HCID 96259 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Diethyl 3-(tert-Butyldimethylsilyloxy)glutarate | HCID 13327289 | — |
Reaktionsschritte
Imidazole and tert-butylchlorodimethylsilane are added to a solution of diethyl 3-hydroxyglutarate in methylene chloride, and the reaction is performed to give diethyl 3-[(tert-butydimethylsilyl)-oxy]pentanedioate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05744604 |
| Quelldatensatz | uspto-grants-1998_04 |
| ORD ID | ord-74225625011f4fc3918d63a785f63c5e |
| Quellennotiz | uspto-grants-1998_04 |