HRID1600351

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID795

Imidazole

C3H4N2

HCID28928

Chloro(1,1-dimethylethyl)dimethylsilane

C6H15ClSi

HCID96259

Diethyl 3-hydroxyglutarate

C9H16O5

PRODUCTS

生成物

结构：CCOC(=O)CC(CC(=O)OCC)O[Si](C)(C)C(C)(C)C

HCID13327289

Diethyl 3-{[tert-butyl(dimethyl)silyl]oxy}pentanedioate

C15H30O5Si

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Imidazole and tert-butylchlorodimethylsilane are added to a solution of diethyl 3-hydroxyglutarate in methylene chloride, and the reaction is performed to give diethyl 3-[(tert-butydimethylsilyl)-oxy]pentanedioate.