Stearic Acid → Octadecanoic acid, silver(1+) salt (1:1)

HRID 16041

Reaktionsgleichung

Reaktionsgleichung von HRID 16041
[C:1]([OH:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[OH-].[Na+].[N+]([O-])([O-])=O.[Ag+:27]>O>[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Ag+:27]

Komponenten

5

Edukt 3

HCID 5281Stearic AcidHCID 14798Sodium HydroxideHCID 24470Silver Nitrate

Produkt 1

HCID 160695Octadecanoic acid, silver(1+) salt (1:1)

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

7.5 g of stearic acid and 1.2 g of sodium hydroxide were added to 300 ml of water and sufficiently stirred until they were completely dissolved. 5.2 g of silver nitrate was added thereto, and the result was stirred for 3 hours. White powder on the surface of the result was collected and washed three times each with distilled water and with methanol to obtain silver stearate. An anode active material was prepared as in Example 1, except that silver stearate was used instead of nickel stearate, the molar ratio of silver to silicon was 0.2:1, the weight ratio of silicon to graphite was 0.5:1, and the carbon layer was 5.2 wt % of the anode active material.

Aufarbeitung

  1. dissolutionwere completely dissolved
  2. stirringthe result was stirred for 3 hours
  3. customWhite powder on the surface of the result was collected
  4. washwashed three times each with distilled water

Quellen und Nachweise

ORD-Eintrag
ord-0f6b71fde1054d1daa9c9fbeee5c6366
Quelldatensatz
uspto-grants-2010_06
Patentnummer
US07736804B2

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