Sodium Methoxide → HCID 19851157, Verbindung

HRID 1606857Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1606857
[CH3:1][NH:2][C:3]1[CH:8]=[C:7](Cl)[CH:6]=[C:5]([NH:10][CH2:11][CH2:12][O:13][CH3:14])[C:4]=1[N+:15]([O-:17])=[O:16].[CH3:18][O-:19].[Na+]>CO>[CH3:1][NH:2][C:3]1[CH:8]=[C:7]([O:19][CH3:18])[CH:6]=[C:5]([NH:10][CH2:11][CH2:12][O:13][CH3:14])[C:4]=1[N+:15]([O-:17])=[O:16]

Komponenten

4

Edukt 2

HCID 10942334Sodium MethoxideHCID 198511582-Methylamino-6-(beta-methoxyethyl)amino-4-chloronitrobenzene

Produkt 1

HCID 19851157HCID 19851157, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.019 mole (5 g) of 2-methylamino-6-(β-methoxyethyl)amino-4-chloronitrobenzene was refluxed with 35 ml of 26% sodium methylate in methanol for 45 minutes then diluted with 100 ml of ice water to precipitate the desired product. Following filtering, water washing and drying under vacuum in the presence of P2O5, the product obtained was recrystallized from isopropanol. It melted at 84° C.

Aufarbeitung

  1. customto precipitate the desired product
  2. filtrationFollowing filtering
  3. dry with materialwater washing and drying under vacuum in the presence of P2O5
  4. customthe product obtained
  5. customwas recrystallized from isopropanol

Quellen und Nachweise

ORD-Eintrag
ord-d58a90feab3246739159828477f4c590
Quelldatensatz
uspto-grants-1989_09
Patentnummer
US04863482

Notizen zur Reaktion

Wird geladen…