5-Methoxytetralone → 5-Methoxy-1,2,3,4-tetrahydronaphthalen-1-amine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	5-Methoxytetralone	HCID 36620	—
Edukt	4,5,6,7-Tetrahydro-1-benzofuran-4-amine	HCID 18525171	—
Produkt	5-Methoxy-1,2,3,4-tetrahydronaphthalen-1-amine	HCID 38899	—

Reaktionsschritte

Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 5-methoxy-3,4-dihydronaphthalen-1(2H)-one and making non-critical variations provided the title compound as a oil: 1H NMR (400 MHz, CDCl3) δ 7.19, 7.05, 6.75, 4.00, 3.84, 2.76, 2.61, 1.97, 1.70; 13C NMR (100 MHz, CDCl3) δ 157.44, 142.83, 126.67, 126.02, 120.53, 108.09, 55.72, 49.75, 33.21, 23.57, 19.11; HRMS (FAB) calcd for C11H15NO+H 178.1232, found 178.1233.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06992087B2
Quelldatensatz	uspto-grants-2006_01
ORD ID	ord-d11a62975fd74a6bb8eea637ab4bbde5
Quellennotiz	uspto-grants-2006_01