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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1620886Erstellt: 26. Oktober 2026

Potassium hydroxy sulfite → 4-{[5-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate

https://huagongshe.com/reaction/1620886

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium hydroxy sulfiteHCID 23707502—
Edukt4-{[5-(Methylsulfanyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetateHCID 57571820—
LösungsmittelChloroformHCID 6212—
Produkt4-{[5-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetateHCID 56969393—

Reaktionsschritte

Using the Oxone® procedure as described in section 1.5.1.7 for the synthesis of compound (I), 515 (0.841 g, 2.73 mmol) gives crude 7. The crude product is stirred with chloroform (50 mL) and the suspension is filtered. The pad is washed once with chloroform and air dried to give pure 7 (0.35 g) as a white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08772502B2
Quelldatensatzuspto-grants-2014_07
ORD IDord-7e3ee9d730574924bdaf720001ab6ccb
Quellennotizuspto-grants-2014_07