HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Tridecyn-1-ol → 1-Bromo-2-tridecyne
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Tridecyn-1-ol | HCID 11116979 | — |
| Edukt | CBr4 triphenylphosphine | HCID 11387777 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 1-Bromo-2-tridecyne | HCID 18673385 | — |
Reaktionsschritte
1-Bromo-2-tridecyne (colorless oil) was prepared from 2-tridecyn-1-ol using the CBr4/triphenylphosphine mixture in dichloromethane to carry out the halogenation. 1-Bromo-2-tridecyne (colorless oil) was thus formed with a yield of 91%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06511670B1 |
| Quelldatensatz | uspto-grants-2003_01 |
| ORD ID | ord-ed1dc395dd2147808413d595d6032b70 |
| Quellennotiz | uspto-grants-2003_01 |