HRID1635774

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11116979

2-TRIDECYN-1-OL

C13H24O

结构：BrC(Br)(Br)Br.c1ccc(P(c2ccccc2)c2ccccc2)cc1

HCID11387777

未命名化合物

PRODUCTS

生成物

HCID18673385

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

1-Bromo-2-tridecyne (colorless oil) was prepared from 2-tridecyn-1-ol using the CBr4/triphenylphosphine mixture in dichloromethane to carry out the halogenation. 1-Bromo-2-tridecyne (colorless oil) was thus formed with a yield of 91%.