HCID 57583245, Verbindung → HCID 57583271, Verbindung
Reaktionsgleichung
[CH2:1]([N:8](C)[CH2:9][CH2:10][CH:11]([CH2:24][N:25](CC1C=CC=CC=1)[CH3:26])[CH2:12][CH2:13][CH2:14][N:15](CC1C=CC=CC=1)[CH3:16])C1C=CC=CC=1.[H][H]>[Pd]>[CH3:1][NH:8][CH2:9][CH2:10][CH:11]([CH2:24][NH:25][CH3:26])[CH2:12][CH2:13][CH2:14][NH:15][CH3:16]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a methanolic solution of N1,N6-Dibenzyl-3-[(benzyl-methyl-amino)-methyl]-N1,N6-dimethylhexane-1,6-diamine (1 g, 0.002 mol) was added 1 g of Pd/C. The solution was exposed to 2 bar of hydrogen and left to shake for 48 hours at ambient temperature. The reaction mixture was filtered through celite and concentrated at reduced pressure to yield a viscous oil. The structure was confirmed by NMR, yield ˜90%.