Ethyl Acetoacetate → 2-(2-Methyl-1,3-dioxan-2-yl)ethanol

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Reaktionsgleichung

[CH2:1]([C:4]1([CH2:10][CH2:11][OH:12])[O:9][CH2:8][CH2:7][CH2:6][O:5]1)CC.C(OCC)(=O)CC(C)=O>>[CH3:1][C:4]1([CH2:10][CH2:11][OH:12])[O:9][CH2:8][CH2:7][CH2:6][O:5]1

Komponenten

Edukt 2

HCID 8868Ethyl Acetoacetate

HCID 597924352-(2-Propyl-1,3-dioxan-2-yl)ethanol

Produkt 1

HCID 596567682-(2-Methyl-1,3-dioxan-2-yl)ethanolAusbeute 49 %

Versuchsvorschrift

The same procedure as in the steps (8a) and (8b) of Example 8, was repeated using ethyl acetoacetate to obtain the title compound (5.4 g, total yield: 49%) as a light yellow oil.

Quellen und Nachweise

ORD-Eintrag: ord-d05fbd205c5e4705a6660212b0b3edf1
Quelldatensatz: uspto-grants-2012_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08124780B2

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