HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → 1-Azaphenanthrene-5,6-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Benzo(F)Quinoline | HCID 6796 | — |
| Edukt | Iodine pentoxide | HCID 159402 | — |
| Produkt | 1-Azaphenanthrene-5,6-dione | HCID 19922456 | — |
Reaktionsschritte
Following the procedure described in Example 608, Part A, 37.5 g (0.153 mole) of commercial 1-azaphenanthrene, 55 g (0.165 mole) of iodine pentoxide in 600 ml glacial acetic acid were refluxed 2 hours. Identical workup yielded 8.4 g, m.p. 215°-216°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05434264 |
| Quelldatensatz | uspto-grants-1995_07 |
| ORD ID | ord-f5b3bdb3f23b4de4adf4a1bf0edc2c7d |
| Quellennotiz | uspto-grants-1995_07 |