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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1649960Erstellt: 26. Oktober 2026

p-Toluenesulfonic acid → 1,1,3,3-tetra(4-[N,N-dimethylamino]phenyl)prop-1-ene

https://huagongshe.com/reaction/1649960

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Eduktp-Toluenesulfonic acidHCID 6101—
EduktMichler's ethyleneHCID 81995—
Edukt4,4'-Bis(dimethylamino)benzhydrolHCID 92742—
LösungsmittelMethanolHCID 887—
Produkt1,1,3,3-tetra(4-[N,N-dimethylamino]phenyl)prop-1-eneHCID 19855551—

Reaktionsschritte

Michler's Ethylene (5g) and of 4,4'-bis-(dimethylamino)-benzhydrol (5g, Michler's Hydrol) were dissolved in methanol (50g) and 4-sulphotoluene (0.1g) was added. After stirring and heating under reflux for 2 hours, the insoluble crude product was isolated by filtration, washed with methanol and crystallised from toluene as a white solid (7g), MP 189°-190° C. It has the structure: ##STR12## Use of TDPP as a colour former in a pressure-sensitive copying paper

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04922020
Quelldatensatzuspto-grants-1990_05
ORD IDord-fef92db789bd46b5a752850ac5aa2b05
Quellennotizuspto-grants-1990_05