Dipotassium Oxalate → Cupric acetate

HRID 1650129

Reaktionsgleichung

Reaktionsgleichung von HRID 1650129
[Cu:1].[Ba].[C:3]([O-])(=O)[C:4]([O-:6])=[O:5].[K+].[K+]>[Y]>[C:4]([O-:6])(=[O:5])[CH3:3].[Cu+2:1].[C:4]([O-:6])(=[O:5])[CH3:3]

Komponenten

5

Edukt 3

HCID 11413Dipotassium OxalateHCID 23978CopperHCID 5355457Barium

Produkt 1

HCID 8895Cupric acetate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 23993YttriumKatalysator

Versuchsvorschrift

The copper, barium, and yttrium solutions were mixed and the potassium oxalate solution was added all at once with vigorous stirring. The pH of the solution was 11.3. A brown gelatinous precipitate formed, and it was filtered, washed thoroughly with water, dried at 120° C., and crushed to a fine powder. The elemental analysis shown in the table below suggested YBa2Cu3 (OH)3 (Ox)2O3.H2O.

Aufarbeitung

  1. customA brown gelatinous precipitate formed
  2. filtrationit was filtered
  3. washwashed thoroughly with water
  4. customdried at 120° C.
  5. customcrushed to a fine powder

Quellen und Nachweise

ORD-Eintrag
ord-e4a56a57932c4e8285f62d692dcb5b68
Quelldatensatz
uspto-grants-1990_05
Patentnummer
US04923849

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