Piperidine → HCID 178431711, Verbindung
Reaktionsgleichung
C1CCNCC1.CC1(C)OC(=O)C(Oc2ccc(Br)cn2)=C1c1ccc(S(C)(=O)=O)cc1>C1CN2CCN1CC2.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.COCCOC.CS(C)=O.F[P-](F)(F)(F)(F)F.Fc1cc(F)c(-c2ccc(C(F)(F)F)cn2)[c]([Ir+][c]2cc(F)cc(F)c2-c2ccc(C(F)(F)F)cn2)c1.[Cl][Ni][Cl]>CC1(C)OC(=O)C(Oc2ccc(N3CCCCC3)cn2)=C1c1ccc(S(C)(=O)=O)cc1Komponenten
7
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 4
Reaktionsbedingungen
- Temperatur
- 55 °C
Aufarbeitung
- additionThe samples was moved from a 1536 well plate into a 384 well plate. The 384 well plate contained 75 microliter of 1% Acetic acid in DMSO solution with 0.003M trimethoxybenzene. The reaction plate was rinsed three times with the same solution to make a total addition volume of ~90 microliters
- aliquot25 microliter of quenched reaction mixture was taken
- additionTo the 25 microliter aliquot 50 microliter of DMSO was added. If the original reaction concentration was 0.05 M (wrt limiting reagent). This would make a final analytical concentration of 0.36 mM which is in line with typical analytical concentrations from this group.
Quellen und Nachweise
- ORD-Eintrag
- ord-cb734ab9d0034dc99ce1c8c57ff8ed27
- Quelldatensatz
- Nano CN PhotoChemistry Informers Library
- Originallink
- Quelle ansehen
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