Glycine → Aluminum Acetate

Temperatur

210 fahrenheit

97.85 g of lemon-flavored hard candy stock was placed in an aluminum pan and heated at 210° F. to a mobile syrup. To this hot stock was added 2.15 g of a dry, finely-ground mixture containing 0.76 g of Al(CH3CO2)3 and 1.39 g of anhydrous glycine, C2H5NO2. The dry component was evenly distributed in the melted stock by thorough mixing and the product was poured onto a greased aluminum pan, forming a circular mass approximately 4 mm thick. As it cooled toward room temperature, it was scored with a lightly greased knife into pieces approximately 1.5 cm square. On cooling to room temperature, the squares were easily broken out of the mass. The yield was 33 pieces with an average weight of 2.4 g. The aluminum content was 1.0 mg per gram and glycine content was 13.9 mg per gram. The molar ratio of glycine to aluminum was 5 to 1. The flavor was very pleasant, without unpleasant aftertaste, and with an astringent mouth-feel.

1. additionTo this hot stock was added 2.15 g of a dry, finely-ground mixture
2. additionby thorough mixing
3. customforming a circular mass approximately 4 mm thick
4. temperatureAs it cooled toward room temperature
5. temperatureOn cooling to room temperature

ORD-Eintrag

ord-175544957fda43a6bc5b3a8f3cdaff25

Quelldatensatz

uspto-grants-1993_10

DOI

10.6084/m9.figshare.5104873.v1

Patentnummer

US05250569