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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1681295Erstellt: 27. Oktober 2026

Liothyronine → N-Bromoacetyl-3,3',5-triiodothyronine

https://huagongshe.com/reaction/1681295

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktLiothyronineHCID 5920—
EduktBromoacetyl bromideHCID 61147—
LösungsmittelEthyl AcetateHCID 8857—
ProduktN-Bromoacetyl-3,3',5-triiodothyronineHCID 122086—

Reaktionsschritte

According to the present invention a solution of 3,3',5-triiodo-L-thyronine and bromoacetyl bromide in ethyl acetate is refluxed for a period of time to produce the bromoacetylated hormone which is then fractionated by high speed countercurrent chromatography to yield highly pure N-bromoacetyl-3,3',5-triiodo-L-thyronine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05169984
Quelldatensatzuspto-grants-1992_12
ORD IDord-5970f06b834348c39766db5e4bc8499b
Quellennotizuspto-grants-1992_12