Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1703848Erstellt: 25. Oktober 2026

N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide

https://huagongshe.com/reaction/1703848

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN,N'-DibutylthioureaHCID 2723622—
EduktBromo-4'-chloro-3'-sulfamoylacetophenoneHCID 12952390—
Produkt3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromideHCID 22760686—

Reaktionsschritte

6.2 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether. Colorless amorphous solid body: decomposition beginning at 100° C., γC=N 1615 cm-1.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04125614
Quelldatensatzuspto-grants-1978_11
ORD IDord-537e8ae6f76342a3b1b0dced6e0de0fd
Quellennotizuspto-grants-1978_11