3-Hydroxy-3-methylglutaric acid monoamide methyl ester → 3-Hydroxy-3-methylglutaric acid monoamide

HRID 1706595Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1706595
C[O:2][C:3](=[O:12])[CH2:4][C:5]([OH:11])([CH3:10])[CH2:6][C:7]([NH2:9])=[O:8]>[OH-].[Na+].O>[OH:11][C:5]([CH3:10])([CH2:4][C:3]([OH:12])=[O:2])[CH2:6][C:7]([NH2:9])=[O:8]

Komponenten

4

Edukt 1

HCID 443709073-Hydroxy-3-methylglutaric acid monoamide methyl ester

Produkt 1

HCID 127207103-Hydroxy-3-methylglutaric acid monoamide

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 962WaterLösungsmittelHCID 14798Sodium HydroxideLösungsmittel

Versuchsvorschrift

1.56 g. (0.01 moles) of 3-hydroxy-3-methylglutaric acid monoamide methyl ester is dissolved in 10 ml of 1 N sodium hydroxide. After 24 hours at room temperature the solution is diluted to 50 ml with water and passed through a 50 ml column of Dowex 50 (H30 ) resin. The column is washed with 100 ml of water and the washings collected and evaporated to afford 3-hydroxy-3-methylglutaric acid monoamide.

Aufarbeitung

  1. washThe column is washed with 100 ml of water
  2. customthe washings collected
  3. customevaporated

Quellen und Nachweise

ORD-Eintrag
ord-7ec5e3fb01bf4664b95d187d6887daf5
Quelldatensatz
uspto-grants-1980_06
Patentnummer
US04208204

Notizen zur Reaktion

Wird geladen…