HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrazine → 5-(4-Chlorophenyl)-2-hydrazinopyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrazine | HCID 9321 | — |
| Edukt | 2-Chloro-5-(4-chlorophenyl)pyridine | HCID 10036554 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | 5-(4-Chlorophenyl)-2-hydrazinopyridine | HCID 20300092 | — |
Reaktionsschritte
A mixture of 21.1 g. of 2-chloro-5-(4-chlorophenyl)-pyridine and 19.5 g. of 95% hydrazine in 200 ml. of pyridine is heated at reflux temperature for 48 hours. The reaction mixture is cooled, poured into an ice-water mixture and filtered. The solid is collected, washed with water and air dried to yield 17.0 g. of the product of the Example as a tan solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04209626 |
| Quelldatensatz | uspto-grants-1980_06 |
| ORD ID | ord-a8ba317649b14c98b8e63a20560f56f6 |
| Quellennotiz | uspto-grants-1980_06 |