Water → 4-N,N-dimethylaminophenylacetic acid

HRID 1721695

Reaktionsgleichung

Reaktionsgleichung von HRID 1721695
[CH3:1][N:2]([CH2:4][CH2:5][CH2:6]C(=C)C(N)=O)[CH3:3].CCl.[C:14](N)(=[O:17])[CH:15]=[CH2:16].N([C:27]([CH3:32])(C)C(N)=N)=NC(C)(C)C(N)=N.[OH2:33]>>[CH3:3][N:2]([C:4]1[CH:5]=[CH:6][C:16]([CH2:15][C:14]([OH:17])=[O:33])=[CH:32][CH:27]=1)[CH3:1]

Komponenten

6

Edukt 5

HCID 962WaterHCID 19692,2'-Diazenediylbis(2-methylpropanimidamide)HCID 6327Methyl ChlorideHCID 6579AcrylamideHCID 18359659Dimethylaminopropylacrylamide

Produkt 1

HCID 1522034-N,N-dimethylaminophenylacetic acid

Versuchsvorschrift

CH3CL/dimethylaminopropylacrylamide, quaternized with methyl chloride, and 29 g of acrylamide were added to 541 g of water with 200 mg azo-bisisobutyroamidine (AIBA) and after passage of nitrogen therethrough, the mixture was irradiated for 30 minutes by an Osram HWL 250-W lamp. The gel so obtained was dried to a residual water content of 9% and ground.

Aufarbeitung

  1. customThe gel so obtained
  2. dry with materialwas dried to a residual water content of 9% and ground

Quellen und Nachweise

ORD-Eintrag
ord-9d73673d2a234ac0a697386f14946bf3
Quelldatensatz
uspto-grants-1996_04
Patentnummer
US05512646

Verknüpfte Notizen

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