Carbon Dioxide → HCID 54358079, Verbindung

HRID 1735947Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1735947
[CH2:1]([O:3][C:4](=[O:37])[C:5](=[NH:36])[CH:6](P(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[C:38](=O)=[O:39]>>[CH2:1]([O:3][C:4](=[O:37])[CH:5]([N:36]=[C:38]=[O:39])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

Komponenten

3

Edukt 2

HCID 280Carbon DioxideHCID 178472716HCID 178472716, Verbindung

Produkt 1

HCID 54358079HCID 54358079, Verbindung

Reaktionsbedingungen

Temperatur
50 °C

Versuchsvorschrift

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

Aufarbeitung

  1. customcondensed into the bomb
  2. customThe bomb is sealed
  3. temperatureThe bomb is cooled
  4. customThe solution is transferred from the bomb to a flask
  5. customas is in the next reaction (Example 11)

Quellen und Nachweise

ORD-Eintrag
ord-faeadfd5a0604f41986fed3e3c12fa5d
Quelldatensatz
uspto-grants-1996_07
Patentnummer
US05539082

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