Acetic Anhydride → N'-acetyl-4-bromo-3-methyl-benzohydrazide

HRID 1741066Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1741066
[Br:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([NH:8][NH2:9])=[O:7])=[CH:4][C:3]=1[CH3:12].[C:13](OC(=O)C)(=[O:15])[CH3:14]>>[C:13]([NH:9][NH:8][C:6](=[O:7])[C:5]1[CH:10]=[CH:11][C:2]([Br:1])=[C:3]([CH3:12])[CH:4]=1)(=[O:15])[CH3:14]

Komponenten

3

Edukt 2

HCID 7918Acetic AnhydrideHCID 39058874-Bromo-3-methylbenzohydrazide

Produkt 1

HCID 21833789N'-acetyl-4-bromo-3-methyl-benzohydrazide

Versuchsvorschrift

4-Bromo-3-methylbenzoic hydrazide (D30, 7.5 g) was suspended in acetic anhydride (7 ml) giving rise to an exothermic reaction. The reaction mixture was cooled to room temperature and the product collected. The solid was washed with ethanol and diethyl ether to afford the title compound as a white powder (5.5 g).

Aufarbeitung

  1. customgiving rise
  2. customto an exothermic reaction
  3. customthe product collected
  4. washThe solid was washed with ethanol and diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-e155852771c64c7daa61ba8f5c1c9111
Quelldatensatz
uspto-grants-1999_10
Patentnummer
US05972951

Notizen zur Reaktion

Wird geladen…