Cyclohexanone → N-Cyclohexyl-N'-dodecyl-1,3-propanediamine

Reaktionsgleichung

[CH2:1]([NH:13][CH2:14][CH2:15][CH2:16][NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[C:18]1(=O)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1>>[CH:18]1([NH:17][CH2:16][CH2:15][CH2:14][NH:13][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1

Komponenten

Edukt 2

HCID 7967Cyclohexanone

HCID 79670Lauraminopropylamine

Produkt 1

HCID 18952691N-Cyclohexyl-N'-dodecyl-1,3-propanediamine

Versuchsvorschrift

Following the general procedure of Example 33, but starting with N-dodecyl-1,3-propanediamine and cyclohexanone, the title compound is produced; IR nmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2)

Quellen und Nachweise

ORD-Eintrag: ord-23138e31417c4a8fbaaced22e32e1376
Quelldatensatz: uspto-grants-1994_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05334712

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