Calcium Carbonate → Phytate

HRID 1743351

Reaktionsgleichung

Reaktionsgleichung von HRID 1743351
C(=O)([O-])[O-].[Ca+2].[C@@H:6]1([O:37][P:38]([OH:41])([OH:40])=[O:39])[C@@H:11]([O:12][P:13]([OH:16])([OH:15])=[O:14])[C@H:10]([O:17][P:18]([OH:21])([OH:20])=[O:19])[C@@H:9]([O:22][P:23]([OH:26])([OH:25])=[O:24])[C@@H:8]([O:27][P:28]([OH:31])([OH:30])=[O:29])[C@H:7]1[O:32][P:33]([OH:36])([OH:35])=[O:34]>>[CH:8]1([O:27][P:28]([OH:31])([OH:30])=[O:29])[CH:9]([O:22][P:23]([OH:25])([OH:26])=[O:24])[CH:10]([O:17][P:18]([OH:20])([OH:21])=[O:19])[CH:11]([O:12][P:13]([OH:16])([OH:15])=[O:14])[CH:6]([O:37][P:38]([OH:41])([OH:40])=[O:39])[CH:7]1[O:32][P:33]([OH:35])([OH:36])=[O:34]

Komponenten

3

Edukt 2

HCID 10112Calcium CarbonateHCID 178527091HCID 178527091, Verbindung

Produkt 1

HCID 890Phytate

Versuchsvorschrift

The new chemical compound is produced by: (1) slowly adding 0.33 kg of calcium carbonate in increments of 0.1 kg to 0.87 kg of phytic acid liquid; (2) heating and refluxing for one hour at 90 degrees Celsius; (3) separating the two solids by filtration; (4) gathering the white solid, which is calcium phytate; (5) dissolving 1 kg of calcium phytate into 2.0 liters of water; (6) heating to 89 degrees Celsius for 10–15 minutes until calcium phytate is dissolved in solution; (7) adding and stirring 0.90 kg of citric acid to solution until dissolved in solution; (8) removing heat source and setting solution in a refrigerated environment at a temperature of 5–10 degrees Celsius allowing crystallization for approximately 6 to 8 hours or until crystallization has ceased; (9) allowing the mixture to dry out at room temperature (75 degrees Celsius) until no liquid is visible, and (10) spreading crystals into a drying pan for approximately 24 hours at a temperature of no more than 40 degrees Celsius yielding approximately 1.2 kg of hexa-citrated phytate.

Aufarbeitung

  1. temperaturerefluxing for one hour at 90 degrees Celsius
  2. custom(3) separating the two solids
  3. filtrationby filtration
  4. dissolution(5) dissolving 1 kg of calcium phytate into 2.0 liters of water
  5. temperature(6) heating to 89 degrees Celsius for 10–15 minutes until calcium phytate
  6. dissolutionis dissolved in solution
  7. addition(7) adding
  8. dissolutionuntil dissolved in solution
  9. custom(8) removing
  10. temperatureheat source
  11. customat a temperature of 5–10 degrees Celsius
  12. customcrystallization for approximately 6 to 8 hours
  13. customuntil crystallization
  14. customto dry out at room temperature (75 degrees Celsius) until no liquid
  15. customfor approximately 24 hours
  16. customat a temperature of no more than 40 degrees Celsius

Quellen und Nachweise

ORD-Eintrag
ord-9078715a26b04a8794fcdc66b0a99876
Quelldatensatz
uspto-grants-2006_03
Patentnummer
US07009067B2

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