Hydroxylamine → 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime

HRID 1747070

Reaktionsgleichung

Reaktionsgleichung von HRID 1747070
[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=O)[CH3:10])[CH:6]=[CH:5][CH:4]=1.[NH2:12][OH:13]>C(O)C>[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=[N:12][OH:13])[CH3:10])[CH:6]=[CH:5][CH:4]=1

Komponenten

4

Edukt 2

HCID 787HydroxylamineHCID 103294471-(6-(Hydroxymethyl)pyridin-2-yl)ethanone

Produkt 1

HCID 1363463671-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.

Aufarbeitung

  1. concentrationThe reaction solution was concentrated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-cbce93e8394845eaade63b03730db94c
Quelldatensatz
uspto-grants-2015_10
Patentnummer
US09150541B2

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