HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cadmium Nitrate → Tetradecanoic acid, cadmium salt (2:1)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cadmium Nitrate | HCID 25154 | — |
| Edukt | Sodium Myristate | HCID 23693095 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Tetradecanoic acid, cadmium salt (2:1) | HCID 66290 | — |
Reaktionsschritte
A solution of cadmium nitrate in methanol was added to a solution of sodium myristate, also in methanol. To obtain high quality cadmium myristate, the sodium myristate solution was heated to about 90° C. until all of the particles are dissolved. Afterward, the cadmium nitrate solution was injected slowly, drop-wise, and the reaction was allowed to take place. The temperature was then reduced to room temperature where the cadmium myristate powder began to precipitate below 65° C. The powder was then collected, filtered, and dried in a box oven. The dried cake was then crushed to produce fine particles of cadmium myristate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09151668B1 |
| Quelldatensatz | uspto-grants-2015_10 |
| ORD ID | ord-9ece35995482423c8ecc348f9e5f9a29 |
| Quellennotiz | uspto-grants-2015_10 |