HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,2'-((1-Methylethylidene)bis(cyclohexane-4,1-diyloxymethylene))bisoxirane → 2,2-Bis{4-[2-hydroxy-3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)propoxy]cyclohexyl}propane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,2'-((1-Methylethylidene)bis(cyclohexane-4,1-diyloxymethylene))bisoxirane | HCID 114514 | — |
| Edukt | 2,2,6,6-Tetramethyl-4-piperidyl benzoate | HCID 579967 | — |
| Produkt | 2,2-Bis{4-[2-hydroxy-3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)propoxy]cyclohexyl}propane | HCID 20510564 | — |
Reaktionsschritte
A mixture of 30.0 g of 4-benzoyloxy-2,2,6,6-tetramethylpiperidine and 15.0 g of 2,2-bis[4-(2,3-epoxypropoxy)cyclohexyl]propane was reacted folowing the procedure described in Example 5, giving the desired Compound No. 78 in the form of a colourless, viscous liquid. The Compound had an Rf value of 0.70 on thin-layer chromatography on silica gel developed with a 15:5:1 by volume mixture of n-hexane, triethylamine and ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04371644 |
| Quelldatensatz | uspto-grants-1983_02 |
| ORD ID | ord-8d6e96003f9a4665b6184f1f8fc1b214 |
| Quellennotiz | uspto-grants-1983_02 |