3-(Methylsulfanyl)propanenitrile → HCID 178458073, Verbindung

HRID 1762976

Reaktionsgleichung

Reaktionsgleichung von HRID 1762976
CSCCC#N.C1SC(NC(N)=N)=NC=1CS[CH2:18][CH2:19][C:20]([NH:22][S:23]([NH2:26])(=[O:25])=[O:24])=[NH:21]>>[S:23]([NH:22][C:20](=[NH:21])[CH:19]=[CH2:18])(=[O:25])(=[O:24])[NH2:26]

Komponenten

3

Edukt 2

HCID 5483863-(Methylsulfanyl)propanenitrileHCID 178418935HCID 178418935, Verbindung

Produkt 1

HCID 178458073HCID 178458073, Verbindung

Versuchsvorschrift

N-sulfamyl-acrylamidine was prepared by a four-step procedure from 3-(methylthio)-propionitrile, with an extremely low (5.5%) yield in several days. The products of the subsequent steps, including famotidine, were isolated by column chromatography.

Aufarbeitung

  1. customyield in several days
  2. customwere isolated by column chromatography

Quellen und Nachweise

ORD-Eintrag
ord-09fcdf6f02f84672bde87c942a1f3963
Quelldatensatz
uspto-grants-1989_05
Patentnummer
US04835281

Verknüpfte Notizen

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