Sulfamide → HCID 178479209, Verbindung

HRID 1762977

Reaktionsgleichung

Reaktionsgleichung von HRID 1762977
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]

Komponenten

4

Edukt 2

HCID 82267SulfamideHCID 867420433-Chloropropionitrile hydrogen chloride

Produkt 1

HCID 178479209HCID 178479209, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 3283Diethyl EtherLösungsmittel

Versuchsvorschrift

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

Aufarbeitung

  1. additionTo a stirred suspension of 9.61 g
  2. filtrationthe product is filtered off
  3. washwashed twice with acetone
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-6ec711e95d084ee185c242200ab7ae81
Quelldatensatz
uspto-grants-1989_05
Patentnummer
US04835281

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