Isopropylamine → 5-Bromo-2-isopropylisoindolin-1-one

HRID 1778735Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1778735
[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([O-:8])=O)=[C:4]([CH2:11]Br)[CH:3]=1.[CH:13]([NH2:16])([CH3:15])[CH3:14]>>[Br:1][C:2]1[CH:3]=[C:4]2[C:5](=[CH:9][CH:10]=1)[C:6](=[O:8])[N:16]([CH:13]([CH3:15])[CH3:14])[CH2:11]2

Komponenten

3

Edukt 2

HCID 6363IsopropylamineHCID 231581454-Bromo-2-(bromomethyl)benzoate

Produkt 1

HCID 117086345-Bromo-2-isopropylisoindolin-1-one

Versuchsvorschrift

This compound was prepared by using procedures analogous to those described for the synthesis of Example 52, Step 6 starting from 4-bromo-2-(bromomethyl)benzoate (AstaTech Cat. No. 27012) and isopropylamine (Aldrich Cat No. 471291). LCMS (M+H)+=254.0/256.0.

Aufarbeitung

  1. customThis compound was prepared

Quellen und Nachweise

ORD-Eintrag
ord-32c92087f00b491cb7501428e1e7979a
Quelldatensatz
uspto-grants-2016_02
Patentnummer
US09266892B2

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