Triethylamine hydrochloride → Triethylammonium tetrakis(pentafluorophenyl)borate

HRID 1780042Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1780042
[F:1][C:2]1[C:7]([B-:8]([C:31]2[C:36]([F:37])=[C:35]([F:38])[C:34]([F:39])=[C:33]([F:40])[C:32]=2[F:41])([C:20]2[C:25]([F:26])=[C:24]([F:27])[C:23]([F:28])=[C:22]([F:29])[C:21]=2[F:30])[C:9]2[C:14]([F:15])=[C:13]([F:16])[C:12]([F:17])=[C:11]([F:18])[C:10]=2[F:19])=[C:6]([F:42])[C:5]([F:43])=[C:4]([F:44])[C:3]=1[F:45].[Li+].Cl.[CH2:48]([N:50]([CH2:53][CH3:54])[CH2:51][CH3:52])[CH3:49]>O>[F:37][C:36]1[C:31]([B-:8]([C:9]2[C:14]([F:15])=[C:13]([F:16])[C:12]([F:17])=[C:11]([F:18])[C:10]=2[F:19])([C:7]2[C:6]([F:42])=[C:5]([F:43])[C:4]([F:44])=[C:3]([F:45])[C:2]=2[F:1])[C:20]2[C:21]([F:30])=[C:22]([F:29])[C:23]([F:28])=[C:24]([F:27])[C:25]=2[F:26])=[C:32]([F:41])[C:33]([F:40])=[C:34]([F:39])[C:35]=1[F:38].[CH2:48]([NH+:50]([CH2:53][CH3:54])[CH2:51][CH3:52])[CH3:49]

Komponenten

4

Edukt 2

HCID 11130Triethylamine hydrochlorideHCID 23709652Lithium tetrakis(pentafluorophenyl)borate

Produkt 1

HCID 11735403Triethylammonium tetrakis(pentafluorophenyl)borateAusbeute 80 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Further, lithium tetrakis(pentafluorophenyl)borate (16 mmol) was reacted with triethylamine hydrochloride (16 mmol) in water to obtain 12.8 mmol of triethylammonium tetrakis(pentafluorophenyl)borate as a white solid product.

Quellen und Nachweise

ORD-Eintrag
ord-3460114c4379446ba9c68a5d70c622a2
Quelldatensatz
uspto-grants-1997_05
Patentnummer
US05629398

Notizen zur Reaktion

Wird geladen…