Butyl iodide → HCID 22218299, Verbindung

Reaktionsgleichung

[Br:1][C:2]1[C:3]([OH:17])=[CH:4][C:5]2[C:6]([CH3:16])([CH3:15])[CH2:7][CH:8]=[C:9]([CH:12]([CH3:14])[CH3:13])[C:10]=2[CH:11]=1.I[CH2:19][CH2:20][CH2:21][CH3:22]>>[Br:1][C:2]1[CH:11]=[C:10]2[C:5](=[CH:4][C:3]=1[O:17][CH2:19][CH2:20][CH2:21][CH3:22])[C:6]([CH3:15])([CH3:16])[CH2:7][CH:8]=[C:9]2[CH:12]([CH3:13])[CH3:14]

Komponenten

Edukt 2

HCID 10962Butyl iodide

HCID 22218215HCID 22218215, Verbindung2×

Produkt 1

HCID 22218299HCID 22218299, VerbindungAusbeute 66 %

Versuchsvorschrift

Following General Procedure O, 3-bromo-5-isopropyl-8,8-dimethyl-7,8-dihydronaphthalen-2-ol (Compound 97, 0.36 g, 1.2 mmol) was reacted with 1-iodobutane to afford 0.28 g (66%) of the title compound as a clear oil.

Quellen und Nachweise

ORD-Eintrag: ord-68830afc9b784007a8e713521c0c7643
Quelldatensatz: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07026487B2

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