1-Methylimidazole → 1-Hexadecyl-3-methylimidazolium Chloride

HRID 1819515Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1819515
[Cl:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17].[CH3:18][N:19]1[CH:23]=[CH:22][N:21]=[CH:20]1>>[Cl-:1].[CH3:18][N+:19]1[CH:23]=[CH:22][N:21]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH:20]=1

Komponenten

3

Edukt 2

HCID 13901-MethylimidazoleHCID 209931-Chlorohexadecane

Produkt 1

HCID 27342311-Hexadecyl-3-methylimidazolium Chloride

Versuchsvorschrift

The procedure of Example 1 was repeated with minor changes. 868 g of 1-chlorohexadecane and 570 g of 1-methylimidazole were added into a 2000 ml three-neck round-bottom flask. The reaction temperature was set from 95 to 100° C. After four hours the milk-like solution transferred into homogenous solution. The reaction was continued for three days. Then, the product was washed with ethyl acetate five times and toluene three times. After that, it was dried under vacuum for three days.

Aufarbeitung

  1. customwas set from 95 to 100° C
  2. waitThe reaction was continued for three days
  3. washThen, the product was washed with ethyl acetate five times and toluene three times
  4. customAfter that, it was dried under vacuum for three days

Quellen und Nachweise

ORD-Eintrag
ord-d9214cb717424488bbed2565859025e2
Quelldatensatz
uspto-grants-2009_10
Patentnummer
US07601772B2

Notizen zur Reaktion

Wird geladen…