HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Hydroxydiphenyl ether → 3-{2-Methyl-4-[3-(2-phenoxy-phenoxy)-phenoxy]-phenyl}-propionic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Hydroxydiphenyl ether | HCID 75491 | — |
| Edukt | 3-[4-(3-Bromo-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester | HCID 57894192 | — |
| Produkt | 3-{2-Methyl-4-[3-(2-phenoxy-phenoxy)-phenoxy]-phenyl}-propionic acid | HCID 11154902 | — |
Reaktionsschritte
The title compound is prepared by reacting the compound of 3-[4-(3-bromo-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester with 2-phenoxy-phenol as in Example 18 to afford 0.106 g (42%). 1H NMR (400 MHz, CDCl3); MS (ES+) m/z mass calculated for C28H24O5 440, found 441 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07608639B2 |
| Quelldatensatz | uspto-grants-2009_10 |
| ORD ID | ord-bbb5588f6e33425e8f85ff4afa165d41 |
| Quellennotiz | uspto-grants-2009_10 |